By Michael B. Smith
ISBN-10: 0471049239
ISBN-13: 9780471049234
ISBN-10: 047135550X
ISBN-13: 9780471355502
ISBN-10: 0471355518
ISBN-13: 9780471355519
ISBN-10: 0471367524
ISBN-13: 9780471367529
ISBN-10: 0471607134
ISBN-13: 9780471607137
ISBN-10: 0471848964
ISBN-13: 9780471848967
ISBN-10: 0471867284
ISBN-13: 9780471867289
Content material: Preface. Abbreviations. Index, Monofunctional Compounds. Index, Difunctional Compounds. creation. 1 guidance of Alkynes. 2 coaching of Acid Derivatives. three instruction of Alcohols. four arrangements of Aldehydes. five practise of Alkyls, Methylens, and Aryls. 6 training of Amides. 7 coaching of Amines. eight education of Esters. nine education of Ethyl Epoxides and Thioethers. 10 coaching of Halides and Sulfonates. eleven practise of Hydrides. 12 instruction of Ketones. thirteen training of Nitriles. 14 training of Alkenes. 15 practise of Oxides. sixteen education of Difunctional Compounds. writer Index
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1988, 53, 1231 95% SECTDN 4 2 A Alcohols From Ketones Bakers Yeast , aq. KOH H ! ; Fuiisawa. T. , 7989, 30, 381 1. 80% ee , R volne. ; Lellouche, I. , 7989, 30, 5141. C&b ere. P. J. Chem. , Chem. , 1989, 224. REVIEW: "Asymmetric Reductions with Organoborane Reagents" Midland. M. Chem. , 7989, 89, 1553. NON-ASYMMETRIC REDUCTION 42 COMPENDIUM OF ORGANIC SYNTHETIC METHODS VOL 7 w -- SECTION 4 2A -L/ THF,0°C,2h 2. ; saburai. H. J. Org. , 1987, 52,948. ;Tsutsurni, 0. Bull. Chem. , 1987, 60, 3423. 1.
Sibille, S . ; Perichon, J. J. Org. , 7989, 54, 2198. REVIEW: Alkylation of Aldehydes SECTION 3 4 B 23 "Asymmetric Reductions with Organoborane Reagents" Midland. M, Chem. , 7989, 89, 1553. & s p GPh+ qph h 2. CeC13, -780Ct Me 3. PhCHO , -78OC OH 12% 5 3 Yo OH Am. Chem. , 1987, 109, 4710. ; Cohen. T,J. ; . J. Org. , 1987, 52, 135. 1M NaOH PH P h 7 2 OO/ Hosorni. A; Kohra, S . ; Torninaga, Y. J. Chem. ,Chem. , 7987, 1517. 2. Ti&, mcH0 CH2C12. -78OC 3. ; Mordini, A,; Jadde i. , 1987, 28, 965. ; Araki, S .
Watt. S, Synth. , 1988, 18, 1 . SECTION 4 2A COMPENDIUM OF ORGANIC SYNTHETIC METHODS VOL 7 38 1. : Ma-; .. Panaioli, S. Synth. ;Waegell, B. , 1989, 30, 5271, 5275. SECTION 42: ALCOHOLS AND THIOLS FROM KETONES The following reaction types are included in this section: A. Reductions of Ketones to Alcohols B. Alkylations of Ketones, forming Alcohols Coupling of ketones to give diols is found in Section 323 (Alcohol -+ Alcohol). ; Yeschambre. H, J. Org. , 1987, 52, 256. Alcohols From Ketones SECTION 4 2 A Kloekera magna C02Et R NRRLY-1611 > 39 OH R h C 0 2 E t QH + Me i e R Y o 2 E t Me 50 R = Me 50 >95%ee >95°/aee 5 R = Et 95 w/&e >95%9e Buisson.
Compendium of Organic Synthetic Methods -Volume 7 by Michael B. Smith
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